@article{034e44e71fb04e76b3adda8d91148201,
title = "1H-2D-nuclear magnetic resonance applied to the primary structure determination of a novel octasaccharide glycolipid isolated from the spermatozoa of bivalves",
abstract = "High resolution, two-dimensional 1H-n.m.r. spectroscopy has been used to confirm a proposed primary structure of a glycolipid having an octasaccharide head-group. Pure absorption and relay experiments were found to be particularly useful in establishing connectivities in poorly resolved regions of the spectrum. The spectral assignments, which indicate novel linkages including an internal fucopyranosyl residue as well as terminal xylosyl and 4-O-methylglucopyranosyluronic acid groups, add to a growing data base for structural characterization through n.m.r. spectroscopy.",
author = "{Neel Scarsdale}, J. and Prestegard, {James H.} and Susumu Ando and Taro Hori and Yu, {Robert K}",
note = "Funding Information: The authors thank Dr. Dennis Hare for the use of his n.m.r. processing software. The research benefited from instrumentationp rovided through shared instrumentationp rograms of the National Institute of General Medical Sciences (grant GM-32 243 Sl) and the Division of Research Resources of NIH (grant RR 02 379). Funding Information: {\textquoteleft}This work was supported by grants GM-33 225 and NS-11 853 from the National Institutes o?{\textquoteright}Health, and by a predoctoral fellowship (to J.N.S.) from the National Science Foundation. {\textquoteleft}To whom correspondence should be addressed.",
year = "1986",
month = nov,
day = "1",
doi = "10.1016/S0008-6215(00)90132-0",
language = "English (US)",
volume = "155",
pages = "45--56",
journal = "Carbohydrate Research",
issn = "0008-6215",
publisher = "Elsevier BV",
number = "C",
}